Issue 35, 2019
From the journal:

Polymer Chemistry

Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors†

Stephen T. Knox, ORCID logo a   Sam Parkinson,a   Raphael Stonea  and  Nicholas J. Warren ORCID logo *a  

* Corresponding authors

a School of Chemical and Process Engineering, University of Leeds, Woodhouse Lane, Leeds, West Yorkshire
E-mail: n.warren@leeds.ac.uk

Abstract

A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.

Graphical abstract: Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

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Article information

DOI
https://doi.org/10.1039/C9PY00982E
Article type
Communication
Submitted
03 Jul 2019
Accepted
06 Aug 2019
First published
07 Aug 2019

Polym. Chem., 2019,10, 4774-4778

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Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

S. T. Knox, S. Parkinson, R. Stone and N. J. Warren, Polym. Chem., 2019, 10, 4774 DOI: 10.1039/C9PY00982E

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