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Issue 7, 2019
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Palladium-catalyzed intramolecular carboborylation of 1,3-diene and synthesis of ABCD ring of communesins

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Abstract

A palladium-catalyzed intramolecular carboborylation of 1,3-diene has been developed for the synthesis of iminoindolines with a quaternary carbon centre. This method was applied to a substrate bearing several functional groups to afford a complex iminoindoline, which was subsequently converted into an ABCD ring model compound of communesins via an intramolecular Friedel–Crafts-type reaction.

Graphical abstract: Palladium-catalyzed intramolecular carboborylation of 1,3-diene and synthesis of ABCD ring of communesins

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Supplementary files

Article information


Submitted
09 Sep 2018
Accepted
03 Oct 2018
First published
04 Oct 2018

Org. Biomol. Chem., 2019,17, 1731-1735
Article type
Communication

Palladium-catalyzed intramolecular carboborylation of 1,3-diene and synthesis of ABCD ring of communesins

C. Tsukano, M. Nakajima, S. M. Hande and Y. Takemoto, Org. Biomol. Chem., 2019, 17, 1731
DOI: 10.1039/C8OB02224K

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