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Issue 22, 2019
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Electrochemical TEMPO-catalyzed multicomponent C(sp3)–H α-carbamoylation of free cyclic secondary amines

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Abstract

We report here an original electrosynthetic method allowing the straightforward C(sp3)–H α-carbamoylation of free cyclic secondary amines. Based on a TEMPO-catalyzed indirect anodic oxidation and a multicomponent coupling, a wide variety of N-acyl α-carboxamides have been obtained under remarkably mild and sustainable reaction conditions.

Graphical abstract: Electrochemical TEMPO-catalyzed multicomponent C(sp3)–H α-carbamoylation of free cyclic secondary amines

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Publication details

The article was received on 09 Sep 2019, accepted on 10 Oct 2019 and first published on 11 Oct 2019


Article type: Paper
DOI: 10.1039/C9GC03173A
Green Chem., 2019,21, 6194-6199

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    Electrochemical TEMPO-catalyzed multicomponent C(sp3)–H α-carbamoylation of free cyclic secondary amines

    N. Pan, J. Ling, R. Zapata, J. Pulicani, L. Grimaud and M. R. Vitale, Green Chem., 2019, 21, 6194
    DOI: 10.1039/C9GC03173A

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