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Electrochemical TEMPO-Catalyzed Multicomponent C(sp3)-H α-Carbamoylation of Free Cyclic Secondary Amines.

Abstract

We report here an original electrosynthetic method allowing the straightforward C(sp3)-H α-carbamoylation of free cyclic secondary amines. Based on a TEMPO-catalyzed indirect anodic oxidation and a multicomponent coupling, a wide variety of N-acyl α-carboxamides have been obtained in remarkably mild and sustainable reaction conditions.

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Publication details

The article was received on 09 Sep 2019, accepted on 10 Oct 2019 and first published on 11 Oct 2019


Article type: Paper
DOI: 10.1039/C9GC03173A
Green Chem., 2019, Accepted Manuscript

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    Electrochemical TEMPO-Catalyzed Multicomponent C(sp3)-H α-Carbamoylation of Free Cyclic Secondary Amines.

    N. Pan, J. Ling, J. Pulicani, L. Grimaud and M. R. VITALE, Green Chem., 2019, Accepted Manuscript , DOI: 10.1039/C9GC03173A

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