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Synthesis of MIL-53 Thin-films by Vapour-Assisted Conversion

Abstract

A simple method for the preparation of MIL-53 thin-films is reported. By employing a vapour-assisted conversion (VAC) approach we were able to prepare homogeneous MIL-53 films on a variety of glass, silicon or alumina substrates. Our strategy uses a vessel that allows film growth in an environment with a solvent-saturated atmosphere, in this case DMF. The VAC preparative conditions lead to the formation of a homogeneous film of the MOF and avoids the formation of alternative aggregates, such as starting materials. The effect of reaction temperature and time are investigated allowing identification of the optimum conditions to produce good film quality.

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Publication details

The article was received on 17 Oct 2019, accepted on 18 Nov 2019 and first published on 19 Nov 2019


Article type: Paper
DOI: 10.1039/C9CE01644A
CrystEngComm, 2019, Accepted Manuscript

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    Synthesis of MIL-53 Thin-films by Vapour-Assisted Conversion

    J. Warfsmann, B. Tokay and N. R. Champness, CrystEngComm, 2019, Accepted Manuscript , DOI: 10.1039/C9CE01644A

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