Primary cycloalkylimines with a 4 to 8-membered ring were synthesized by dehydrocyanation of the corresponding α-aminonitriles on solid potassium hydroxide via a vacuum gas–solid reaction. Imine–enamine tautomerism has been demonstrated at room temperature for the most kinetically stable derivatives.
J. Guillemin, W. Nasraoui and H. Gazzeh, Chem. Commun., 2019, 55, 5647 DOI: 10.1039/C9CC01755K
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