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Visible-light photocatalytic trifluoromethylthiolation of aryldiazonium salts: conversion of amino group into trifluoromethylthiol group

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Abstract

A visible-light photocatalytic trifluoromethylthiolation of aryl amine through in situ generation of aryldiazonium salts as key intermediates was achieved with S-trifluoromethyl 4-methoxylbenzenesulfonothioate for the first time. The mild reaction conditions and readily accessible reagents provide a practical protocol to prepare aryl trifluoromethylthioether.

Graphical abstract: Visible-light photocatalytic trifluoromethylthiolation of aryldiazonium salts: conversion of amino group into trifluoromethylthiol group

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Publication details

The article was received on 18 Apr 2018, accepted on 26 May 2018 and first published on 28 May 2018


Article type: Research Article
DOI: 10.1039/C8QO00401C
Citation: Org. Chem. Front., 2018, Advance Article
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    Visible-light photocatalytic trifluoromethylthiolation of aryldiazonium salts: conversion of amino group into trifluoromethylthiol group

    X. Zhao, X. Zheng, M. Tian, Y. Tong, B. Yang, X. Wei, D. Qiu and K. Lu, Org. Chem. Front., 2018, Advance Article , DOI: 10.1039/C8QO00401C

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