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Issue 37, 2018
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tert-Butyl nitrite mediated nitrogen transfer reactions: synthesis of benzotriazoles and azides at room temperature

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Abstract

A conversion of o-phenylenediamines into benzotriazoles was achieved at room temperature using tert-butyl nitrite. The optimized conditions are also well suited for the transformation of sulfonyl and acyl hydrazines into corresponding azides. This protocol does not require any catalyst or acidic medium. The desired products were obtained in excellent yields in a short span of time.

Graphical abstract: tert-Butyl nitrite mediated nitrogen transfer reactions: synthesis of benzotriazoles and azides at room temperature

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Publication details

The article was received on 09 Aug 2018, accepted on 07 Sep 2018 and first published on 07 Sep 2018


Article type: Paper
DOI: 10.1039/C8OB01950A
Citation: Org. Biomol. Chem., 2018,16, 8280-8285

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    tert-Butyl nitrite mediated nitrogen transfer reactions: synthesis of benzotriazoles and azides at room temperature

    S. Azeez, P. Chaudhary, P. Sureshbabu, S. Sabiah and J. Kandasamy, Org. Biomol. Chem., 2018, 16, 8280
    DOI: 10.1039/C8OB01950A

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