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Abstract | Cited by

An efficient halogen-free Cs2CO3-promoted methylene insertion into disulfide bonds has been achieved using acetone as a methylene source under mild conditions. This method provides a convenient and practical route to dithioacetals in up to 96% yield with good functional group compatibility.

Graphical abstract: Cs2CO3-promoted methylene insertion into disulfide bonds using acetone as a methylene source

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