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Issue 22, 2018
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An aqueous medium-controlled stereospecific oxidative iodination of alkynes: efficient access to (E)-diiodoalkene derivatives

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Abstract

A new and versatile approach for the stereospecific iodination of alkynes using cheap, air stable and non-toxic reagents in aqueous media has been developed. This protocol is tolerant of various functional groups, and provides a broad range of vicinal diiodoalkenes with exceptional E-selectivity under mild conditions. Scale-up reactions (up to 5 g) established the proficiency of this protocol and highlight the feasibility of large scale reactions.

Graphical abstract: An aqueous medium-controlled stereospecific oxidative iodination of alkynes: efficient access to (E)-diiodoalkene derivatives

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Publication details

The article was received on 04 Aug 2018, accepted on 04 Oct 2018 and first published on 05 Oct 2018


Article type: Letter
DOI: 10.1039/C8NJ03929A
Citation: New J. Chem., 2018,42, 17879-17883
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    An aqueous medium-controlled stereospecific oxidative iodination of alkynes: efficient access to (E)-diiodoalkene derivatives

    R. Banothu, S. Peraka, S. Kodumuri, D. Chevella, K. S. Gajula, V. Amrutham, D. R. Yennamaneni and N. Nama, New J. Chem., 2018, 42, 17879
    DOI: 10.1039/C8NJ03929A

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