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Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

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Abstract

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

Graphical abstract: Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

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Publication details

The article was received on 09 Oct 2018, accepted on 07 Nov 2018 and first published on 07 Nov 2018


Article type: Communication
DOI: 10.1039/C8CC08065H
Citation: Chem. Commun., 2018, Advance Article
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    Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

    K. Motiram-Corral, M. Pérez-Trujillo, P. Nolis and T. Parella, Chem. Commun., 2018, Advance Article , DOI: 10.1039/C8CC08065H

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