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Issue 65, 2017
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Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

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Abstract

2D double-quantum single-quantum correlation spectra with arbitrary spectral widths can be recorded with SR26 and related supercycled recoupling sequences when applying Supercycle-Timing-Compensation (STiC) phase shifts. This concept widely extends the applicability of supercycled sequences, most importantly for obtaining long-range distance constraints for structure determination with solid-state NMR.

Graphical abstract: Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

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Article information


Submitted
23 Jun 2017
Accepted
27 Jul 2017
First published
01 Aug 2017

Chem. Commun., 2017,53, 9155-9158
Article type
Communication

Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

K. Märker, S. Hediger and G. De Paëpe, Chem. Commun., 2017, 53, 9155
DOI: 10.1039/C7CC04890D

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