Clearing the undergrowth: detection and quantification of low level impurities using 19F NMR

Pinelopi Moutzouri; Peter Kiraly; Andrew R. Phillips; Steven R. Coombes; Mathias Nilsson; Gareth A. Morris

doi:10.1039/C6CC08836H

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Clearing the undergrowth: detection and quantification of low level impurities using ¹⁹F NMR

Pinelopi Moutzouri, Peter Kiraly, Andrew R. Phillips, Steven R. Coombes, Mathias Nilsson and Gareth A. Morris
Chem. Commun., 2017,53, 123-125
DOI: 10.1039/C6CC08836H, Communication

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Abstract | Cited by

A new method for the analysis of low level impurities in sparsely fluorinated species allows measurement of clean high dynamic range ¹⁹F spectra, fully decoupled and free of interfering signals from ¹³C isotopomers.

Graphical abstract: Clearing the undergrowth: detection and quantification of low level impurities using 19F NMR

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