Issue 64, 2016, Issue in Progress
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RSC Advances

Palladium-catalyzed direct C–H arylation of ferrocenecarboxamides with aryl halides†

Huijie Qiao,a   Suyan Sun,a   Fan Yang,*a   Yu Zhu,a   Weiguo Zhu,a   Yusheng Wu*bc  and  Yangjie Wu*a  

* Corresponding authors

a The College of Chemistry and Molecular Engineering, Henan Key Laboratory of Chemical Biology and Organic Chemistry, Key Laboratory of Applied Chemistry of Henan Universities, Zhengzhou University, Zhengzhou 450052, People's Republic of China
E-mail: yangf@zzu.edu.cn, wyj@zzu.edu.cn

b Tetranov Biopharm, LLC., 75 Daxue Road, Zhengzhou, People's Republic of China
E-mail: yusheng.wu@tetranovglobal.com

c Collaborative Innovation Center of New Drug Research and Safety Evaluation, Henan Province, PR China
E-mail: yusheng.wu@tetranovglobal.com

Abstract

A simple and facile protocol for the palladium-catalyzed ortho-arylation of ferrocenecarboxamides with aryl halides was developed with the assistance of the bidentate directing group. The substrate scope could be extended to aryl iodides, bromides and even chlorides, as well as heterocyclic halides, affording diarylated products in moderate to good yields.

Graphical abstract: Palladium-catalyzed direct C–H arylation of ferrocenecarboxamides with aryl halides

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Article information

DOI
https://doi.org/10.1039/C6RA11972G
Article type
Paper
Submitted
09 May 2016
Accepted
13 Jun 2016
First published
13 Jun 2016

RSC Adv., 2016,6, 59319-59326

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Palladium-catalyzed direct C–H arylation of ferrocenecarboxamides with aryl halides

H. Qiao, S. Sun, F. Yang, Y. Zhu, W. Zhu, Y. Wu and Y. Wu, RSC Adv., 2016, 6, 59319 DOI: 10.1039/C6RA11972G

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