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Issue 21, 2016
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Synthetic investigation toward apigenin 5-O-glycoside camellianin B as well as the chemical structure revision

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Abstract

Capitalizing on the Au(I)-catalyzed ortho-alkynylbenzoate glycosylation method, the first total synthesis of the proposed structure of apigenin-5-O-glycoside camellianin B was achieved, wherein three approaches, one linear and two convergent, were established, through which the synthetic structures were firmly corroborated. Meanwhile, through the synthesis of anthentic camellianin B via commercially available camellianin A, the misassigned structures of camellianins A and B were revised.

Graphical abstract: Synthetic investigation toward apigenin 5-O-glycoside camellianin B as well as the chemical structure revision

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Publication details

The article was received on 26 Mar 2016, accepted on 18 Apr 2016 and first published on 19 Apr 2016


Article type: Paper
DOI: 10.1039/C6OB00655H
Org. Biomol. Chem., 2016,14, 4842-4847

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    Synthetic investigation toward apigenin 5-O-glycoside camellianin B as well as the chemical structure revision

    Y. Hu, Y. Tu, D. Liu, J. Liao and J. Sun, Org. Biomol. Chem., 2016, 14, 4842
    DOI: 10.1039/C6OB00655H

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