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Issue 36, 2016
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Total synthesis based on the originally claimed structure of mucosin

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Abstract

The first total synthesis aimed at the naturally occurring eicosanoid bicycle mucosin is reported. A practical route has been devised allowing the issues relating to the previous assignment of stereochemistry to be examined. X-ray crystallography was performed on a late stage intermediate to pinpoint the topological relationship displayed by the featured bicyclo[4.3.0]non-3-ene scaffold.

Graphical abstract: Total synthesis based on the originally claimed structure of mucosin

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Article information


Submitted
15 Jul 2016
Accepted
09 Aug 2016
First published
09 Aug 2016

Org. Biomol. Chem., 2016,14, 8433-8437
Article type
Communication

Total synthesis based on the originally claimed structure of mucosin

H. C. Gallantree-Smith, S. G. Antonsen, C. H. Görbitz, T. V. Hansen, J. M. J. Nolsøe and Y. H. Stenstrøm, Org. Biomol. Chem., 2016, 14, 8433
DOI: 10.1039/C6OB01511E

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