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Issue 43, 2016
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bcTol: a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules

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Abstract

Dynamic nuclear polarization (DNP) is an efficient method to overcome the inherent low sensitivity of magic-angle spinning (MAS) solid-state NMR. We report a new polarizing agent (bcTol), designed for biological applications, that yielded an enhancement value of 244 in a microcrystalline SH3 domain sample at 110 K.

Graphical abstract: bcTol: a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules

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Publication details

The article was received on 29 Feb 2016, accepted on 03 May 2016 and first published on 10 May 2016


Article type: Communication
DOI: 10.1039/C6CC01813K
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Chem. Commun., 2016,52, 7020-7023

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    bcTol: a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules

    A. P. Jagtap, M. Geiger, D. Stöppler, M. Orwick-Rydmark, H. Oschkinat and S. Th. Sigurdsson, Chem. Commun., 2016, 52, 7020
    DOI: 10.1039/C6CC01813K

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