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Issue 113, 2015
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Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

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Abstract

The mild and efficient deuteration of terminal alkynes (mono-substituted alkynes) proceeded in the presence of a basic anion exchange resin, WA30, which is a polystyrene polymer bearing a tertiary amine residue on the aromatic nuclei, in heavy water (D2O) at room temperature. WA30 could be easily removed by a simple filtration and repeatedly reused.

Graphical abstract: Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

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Publication details

The article was received on 15 Sep 2015, accepted on 22 Oct 2015 and first published on 23 Oct 2015


Article type: Communication
DOI: 10.1039/C5RA18921G
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RSC Adv., 2015,5, 92954-92957

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    Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

    T. Yamada, K. Park, Y. Monguchi, Y. Sawama and H. Sajiki, RSC Adv., 2015, 5, 92954
    DOI: 10.1039/C5RA18921G

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