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Issue 41, 2015
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Facile synthesis of a conjugated microporous polymeric monolith via copper-free Sonogashira–Hagihara cross-coupling in water under aerobic conditions

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Abstract

A conjugated microporous polymer was synthesized via a modified Sonogashira–Hagihara cross-coupling reaction under aerobic conditions in water and in the absence of copper. These conditions allowed the directing of the CMP format during synthesis into a monolithic structure. Post-modification of the polymer with thiol–yne chemistry followed by AgI uptake led to a catalytically active material for a heterocyclization reaction.

Graphical abstract: Facile synthesis of a conjugated microporous polymeric monolith via copper-free Sonogashira–Hagihara cross-coupling in water under aerobic conditions

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Publication details

The article was received on 22 May 2015, accepted on 27 May 2015 and first published on 02 Jun 2015


Article type: Communication
DOI: 10.1039/C5PY00772K
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Polym. Chem., 2015,6, 7251-7255

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    Facile synthesis of a conjugated microporous polymeric monolith via copper-free Sonogashira–Hagihara cross-coupling in water under aerobic conditions

    J. Liu, J. M. Tobin, Z. Xu and F. Vilela, Polym. Chem., 2015, 6, 7251
    DOI: 10.1039/C5PY00772K

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