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Issue 70, 2015
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Sealed rotors for in situ high temperature high pressure MAS NMR

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Abstract

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

Graphical abstract: Sealed rotors for in situ high temperature high pressure MAS NMR

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Article information


Submitted
11 May 2015
Accepted
06 Jul 2015
First published
06 Jul 2015

Chem. Commun., 2015,51, 13458-13461
Article type
Communication
Author version available

Sealed rotors for in situ high temperature high pressure MAS NMR

J. Z. Hu, M. Y. Hu, Z. Zhao, S. Xu, A. Vjunov, H. Shi, D. M. Camaioni, C. H. F. Peden and J. A. Lercher, Chem. Commun., 2015, 51, 13458
DOI: 10.1039/C5CC03910J

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