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Issue 7, 2015
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Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

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Abstract

A new method, based on slice-selective NMR spectroscopy of inhomogeneous mixtures, is introduced to perform NMR titrations and reaction monitoring in a single experiment. The method was applied to the titration of a lithium salt with 12-crown-4, and to the reaction of nBuLi with N,N,N′,N′′,N′′-pentamethyldiethylenetriamine (PMDTA).

Graphical abstract: Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

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Publication details

The article was received on 21 Oct 2014, accepted on 28 Nov 2014 and first published on 28 Nov 2014


Article type: Communication
DOI: 10.1039/C4CC08329F
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Chem. Commun., 2015,51, 1275-1277
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    Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

    T. Niklas, D. Stalke and M. John, Chem. Commun., 2015, 51, 1275
    DOI: 10.1039/C4CC08329F

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