Temperature-controlled phase transfer hydrothermal synthesis of MWW zeolites was realized with hexamethyleneimine as a structure-directing agent and aniline as a structure-promoting agent. During crystallization, hexamethyleneimine and aniline were completely soluble. After crystallization with decreased temperature, aniline extracted hexamethyleneimine from the mother liquid to the organic phase for reuse.
E. Xing, X. Gao, W. Xie, F. Zhang, X. Mu and X. Shu, RSC Adv., 2014, 4, 24893 DOI: 10.1039/C4RA02678K
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