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Issue 92, 2014
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A facile single crystal to single crystal transition with significant structural contraction on desolvation

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Abstract

5-Ethynyl-1,3-benzenedicarboxylic acid (H2ebdc) reacted with lead(II) acetate trihydrate yields a 1D ladder network, [Pb(ebdc)(MeOH)]2·H2O (1). Removing crystals of 1 from the mother liquor results in a facile single crystal to single crystal transition, yielding 2D [Pb(ebdc)] net (2) with a change in space group from I2/a to P[1 with combining macron].

Graphical abstract: A facile single crystal to single crystal transition with significant structural contraction on desolvation

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Supplementary files

Article information


Submitted
21 Aug 2014
Accepted
26 Sep 2014
First published
01 Oct 2014

This article is Open Access

Chem. Commun., 2014,50, 14436-14439
Article type
Communication
Author version available

A facile single crystal to single crystal transition with significant structural contraction on desolvation

J. V. Knichal, W. J. Gee, A. D. Burrows, P. R. Raithby, S. J. Teat and C. C. Wilson, Chem. Commun., 2014, 50, 14436
DOI: 10.1039/C4CC06587E

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