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Issue 17, 2014
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Temperature-programmed reduction of NiO nanoparticles followed by time-resolved RIXS

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Abstract

The electronic structure of nano-NiO was determined using resonant inelastic X-ray scattering (RIXS) spectroscopy. The nanosized NiO particles were reduced in situ, leading to the formation of metallic Ni in a single step. Time-resolved RIXS elucidated in real time the changes on the occupied and unoccupied electronic structure of the material, which are dramatically affected by the reduction process.

Graphical abstract: Temperature-programmed reduction of NiO nanoparticles followed by time-resolved RIXS

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Supplementary files

Article information


Submitted
01 Nov 2013
Accepted
03 Dec 2013
First published
16 Dec 2013

Phys. Chem. Chem. Phys., 2014,16, 7692-7696
Article type
Communication

Temperature-programmed reduction of NiO nanoparticles followed by time-resolved RIXS

J. Sá, Y. Kayser, C. J. Milne, D. L. Abreu Fernandes and J. Szlachetko, Phys. Chem. Chem. Phys., 2014, 16, 7692
DOI: 10.1039/C3CP54622E

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