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Issue 9, 2014
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Syntheses of, and structural studies on, benzo-fused 1,2,4-thiadiazines

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Abstract

The syntheses of nine benzo-fused-1,2,4-thiadizines are reported. The use of microwave synthesis has been shown to afford high yields and short reaction times in several key reaction steps. The molecular geometries of these heterocycles are discussed and their solid state packing motifs reveal a strong tendency for the N–H group to form hydrogen bonded chains.

Graphical abstract: Syntheses of, and structural studies on, benzo-fused 1,2,4-thiadiazines

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Article information


Submitted
30 Oct 2013
Accepted
24 Dec 2013
First published
07 Jan 2014

CrystEngComm, 2014,16, 1755-1762
Article type
Paper

Syntheses of, and structural studies on, benzo-fused 1,2,4-thiadiazines

E. R. Clark, J. J. Hayward, B. J. Leontowicz, D. J. Eisler and J. M. Rawson, CrystEngComm, 2014, 16, 1755
DOI: 10.1039/C3CE42205D

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