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Issue 23, 2014
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Template-induced polymorphic selectivity: the effects of surface chemistry and solute concentration on carbamazepine crystallisation

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Abstract

Cooling crystallisation of carbamazepine solution in glass vials functionalised with different silane molecules resulted in preferential nucleation of metastable form II or stable form III polymorphs within a definite range of supersaturation. In contrast, the two crystal forms nucleated concomitantly on a control substrate under similar solution conditions.

Graphical abstract: Template-induced polymorphic selectivity: the effects of surface chemistry and solute concentration on carbamazepine crystallisation

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Article information


Submitted
24 Dec 2013
Accepted
04 Mar 2014
First published
04 Mar 2014

CrystEngComm, 2014,16, 4927-4930
Article type
Communication
Author version available

Template-induced polymorphic selectivity: the effects of surface chemistry and solute concentration on carbamazepine crystallisation

J. V. Parambil, S. K. Poornachary, R. B. H. Tan and J. Y. Y. Heng, CrystEngComm, 2014, 16, 4927
DOI: 10.1039/C3CE42622J

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