Issue 15, 2015

Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

Abstract

A rapid NMR data acquisition strategy in terms of enhanced resolution per time unit for the simple and efficient determination of multiple coupling constants is described. The use of 13C spectral aliasing combined by broadband 1H homodecoupling allows accurate measurements from ultra high resolved 2D HSQC cross-peaks.

Graphical abstract: Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

Supplementary files

Article information

Article type
Communication
Submitted
23 Dec 2014
Accepted
14 Jan 2015
First published
14 Jan 2015

Chem. Commun., 2015,51, 3262-3265

Author version available

Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

N. Marcó, A. Fredi and T. Parella, Chem. Commun., 2015, 51, 3262 DOI: 10.1039/C4CC10279G

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