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Issue 73, 2014
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High-yield, regiospecific bis-functionalization of C70 using a Diels–Alder reaction in molten anthracene

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Abstract

A regiospecific bis-adduct of C70 with anthracene was prepared with unusually high yield (68%) by the Diels–Alder reaction in the absence of solvent (melt). The structure of the bis-adduct was an unexpected 12 o'clock isomer, as determined by single crystal X-ray diffraction, thermal gravimetric analysis (TGA) and spectroscopy.

Graphical abstract: High-yield, regiospecific bis-functionalization of C70 using a Diels–Alder reaction in molten anthracene

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Supplementary files

Article information


Submitted
03 Apr 2014
Accepted
09 May 2014
First published
09 May 2014

Chem. Commun., 2014,50, 10584-10587
Article type
Communication
Author version available

High-yield, regiospecific bis-functionalization of C70 using a Diels–Alder reaction in molten anthracene

V. S. P. K. Neti, M. R. Cerón, A. Duarte-Ruiz, M. M. Olmstead, A. L. Balch and L. Echegoyen, Chem. Commun., 2014, 50, 10584
DOI: 10.1039/C4CC02472A

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