Issue 30, 2014
From the journal:

Chemical Communications

Direct observation of supported W bis-methylidene from supported W-methyl/methylidyne species†

E. Callens,*a   E. Abou-Hamad,a   N. Riachea  and  J. M. Basset*a  

* Corresponding authors

a KAUST Catalyst Center, Physical Sciences and Engineering Division, King Abdullah University of Science and Technology, Thuwal, Saudi Arabia
E-mail: Emmanuel.callens@kaust.edu.sa, Jean-Marie.Basset@kaust.edu.sa

Abstract

Extensive solid-state NMR analyses unambiguously determine the formation of silica supported W bis-methylidene methyl species by reaction of the corresponding methyl carbyne with trimethylphosphine or a cyclic olefin.

Graphical abstract: Direct observation of supported W bis-methylidene from supported W-methyl/methylidyne species

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Article information

DOI
https://doi.org/10.1039/C4CC00286E
Article type
Communication
Submitted
13 Jan 2014
Accepted
19 Feb 2014
First published
25 Feb 2014

Chem. Commun., 2014,50, 3982-3985

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Direct observation of supported W bis-methylidene from supported W-methyl/methylidyne species

E. Callens, E. Abou-Hamad, N. Riache and J. M. Basset, Chem. Commun., 2014, 50, 3982 DOI: 10.1039/C4CC00286E

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