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Issue 25, 2014
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Enantioselective, intermolecular [2+2] photocycloaddition reactions of 3-acetoxyquinolone: total synthesis of (−)-pinolinone

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Abstract

The natural product (−)-pinolinone was synthesised via a concise route (six steps, 17% overall yield) from 3-acetoxyquinolone, employing an enantioselective intermolecular [2+2] photocycloaddition as the key step.

Graphical abstract: Enantioselective, intermolecular [2+2] photocycloaddition reactions of 3-acetoxyquinolone: total synthesis of (−)-pinolinone

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Supplementary files

Article information


Submitted
13 Dec 2013
Accepted
07 Feb 2014
First published
18 Feb 2014

This article is Open Access

Chem. Commun., 2014,50, 3353-3355
Article type
Communication
Author version available

Enantioselective, intermolecular [2+2] photocycloaddition reactions of 3-acetoxyquinolone: total synthesis of (−)-pinolinone

F. Mayr, C. Wiegand and T. Bach, Chem. Commun., 2014, 50, 3353
DOI: 10.1039/C3CC49469A

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