Jump to main content
Jump to site search

Issue 8, 2013
Previous Article Next Article

Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

Author affiliations

Abstract

The synthesis of a new mesoporous BTD-COF based on a transesterification reaction was carried out in a two step microwave synthesis procedure in only 40 min: first the pinacolboronate 4,7-bis[4-(4,4,5,5)-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzo[1,2,5]-thiadiazole (BTDBE) was cleaved with HCl, in a second step addition of hexahydroxytriphenylene (HHTP) resulted in the growth of the crystalline framework with high surface area and a pore size of about 4 nm.

Graphical abstract: Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

Back to tab navigation

Supplementary files

Article information


Submitted
21 Aug 2012
Accepted
21 Nov 2012
First published
22 Nov 2012

CrystEngComm, 2013,15, 1500-1502
Article type
Communication

Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

M. Dogru, A. Sonnauer, S. Zimdars, M. Döblinger, P. Knochel and T. Bein, CrystEngComm, 2013, 15, 1500
DOI: 10.1039/C2CE26343B

Social activity

Search articles by author

Spotlight

Advertisements