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A general redox procedure was successfully developed for the controlled synthesis of substituted cobalt oxides with hierarchical flower-like nanostructures comprising unique Y-shaped interconnections. The substitution and nanostructures synergistically enhance the material’s electrochemical activities for highly efficient sensing of H2O2.

Graphical abstract: Hierarchical nanostructures with unique Y-shaped interconnection networks in manganese substituted cobalt oxides: the enhancement effect on electrochemical sensing performance

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