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Issue 27, 2012
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Continuous-flow synthesis of activated vitamin D3 and its analogues

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Abstract

An efficient, two-stage, continuous-flow synthesis of 1α,25-(OH)2-vitamin D3 (activated vitamin D3) and its analogues was achieved. The developed method afforded the desired products in satisfactory yields using a high-intensity and economical light source, i.e., a high-pressure mercury lamp. In addition, our method required neither intermediate purification nor high-dilution conditions.

Graphical abstract: Continuous-flow synthesis of activated vitamin D3 and its analogues

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Article information


Submitted
09 Mar 2012
Accepted
24 Apr 2012
First published
25 Apr 2012

Org. Biomol. Chem., 2012,10, 5205-5211
Article type
Paper

Continuous-flow synthesis of activated vitamin D3 and its analogues

S. Fuse, Y. Mifune, N. Tanabe and T. Takahashi, Org. Biomol. Chem., 2012, 10, 5205
DOI: 10.1039/C2OB25511A

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