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Issue 5, 2012
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Nondestructive volumetric 3-D chemical mapping of nickel-sulfur compounds at the nanoscale

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Abstract

Nano-structures of nickel (Ni) and nickel subsulfide (Ni3S2) materials were studied and mapped in 3D with high-resolution x-ray nanotomography combined with full field XANES spectroscopy. This method for characterizing these phases in complex microstructures is an important new analytical imaging technique, applicable to a wide range of nanoscale and mesoscale electrochemical systems.

Graphical abstract: Nondestructive volumetric 3-D chemical mapping of nickel-sulfur compounds at the nanoscale

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Article information


Submitted
09 Nov 2011
Accepted
06 Jan 2012
First published
10 Jan 2012

Nanoscale, 2012,4, 1557-1560
Article type
Communication

Nondestructive volumetric 3-D chemical mapping of nickel-sulfur compounds at the nanoscale

W. M. Harris, G. J. Nelson, A. M. Kiss, J. R. Izzo, Y. Liu, M. Liu, S. Wang, Y. S. Chu and W. K. S. Chiu, Nanoscale, 2012, 4, 1557
DOI: 10.1039/C2NR11690A

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