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Issue 13, 2012
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Metal induced folding: synthesis and conformational analysis of the lanthanide complexes of two 44-membered hydrazone macrocycles

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Abstract

Six new lanthanide complexes of two 44-membered macrocycles have been prepared and characterised in solution. An analysis of the conformations of the free macrocycles and their lanthanide complexes both in solution (2D NMR) and in solid state (X-ray crystallography) demonstrate that the complexation induces changes in folding of the macrocycles.

Graphical abstract: Metal induced folding: synthesis and conformational analysis of the lanthanide complexes of two 44-membered hydrazone macrocycles

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Article information


Submitted
02 Oct 2011
Accepted
12 Jan 2012
First published
15 Feb 2012

Dalton Trans., 2012,41, 3780-3786
Article type
Paper

Metal induced folding: synthesis and conformational analysis of the lanthanide complexes of two 44-membered hydrazone macrocycles

J. M. Klein, J. K. Clegg, V. Saggiomo, L. Reck, U. Lüning and J. K. M. Sanders, Dalton Trans., 2012, 41, 3780
DOI: 10.1039/C2DT11861K

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