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Issue 5, 2012
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Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

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Abstract

Diastereomeric co-crystals of the title compounds display sufficiently different powder diffractograms in order to determine the absolute configuration of one of the two crystal formers. Selective formation of the more stable diastereomer is observed if racemic conglomerates or racemates are subjected to ball-milling.

Graphical abstract: Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

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Article information


Submitted
26 Oct 2011
Accepted
04 Jan 2012
First published
18 Jan 2012

CrystEngComm, 2012,14, 1534-1537
Article type
Communication

Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

D. A. Bock and C. W. Lehmann, CrystEngComm, 2012, 14, 1534
DOI: 10.1039/C2CE06427H

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