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Issue 5, 2012
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Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

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Abstract

Diastereomeric co-crystals of the title compounds display sufficiently different powder diffractograms in order to determine the absolute configuration of one of the two crystal formers. Selective formation of the more stable diastereomer is observed if racemic conglomerates or racemates are subjected to ball-milling.

Graphical abstract: Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

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Publication details

The article was received on 26 Oct 2011, accepted on 04 Jan 2012 and first published on 18 Jan 2012


Article type: Communication
DOI: 10.1039/C2CE06427H
Citation: CrystEngComm, 2012,14, 1534-1537

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    Chirality determination from X-ray powder data—diastereomeric co-crystals of mandelic acid and proline amide

    D. A. Bock and C. W. Lehmann, CrystEngComm, 2012, 14, 1534
    DOI: 10.1039/C2CE06427H

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