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Issue 96, 2012
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Mechanosynthesis of amides in the total absence of organic solvent from reaction to product recovery

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Abstract

The synthesis of various amides has been realised avoiding the use of any organic solvent from activation of carboxylic acids with CDI to isolation of the amides. Mechanochemistry was the key point of the process allowing rapid formation of the amide bond and efficient water-based purification of the final products.

Graphical abstract: Mechanosynthesis of amides in the total absence of organic solvent from reaction to product recovery

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Article information


Submitted
31 Aug 2012
Accepted
08 Oct 2012
First published
29 Oct 2012

Chem. Commun., 2012,48, 11781-11783
Article type
Communication

Mechanosynthesis of amides in the total absence of organic solvent from reaction to product recovery

T. Métro, J. Bonnamour, T. Reidon, J. Sarpoulet, J. Martinez and F. Lamaty, Chem. Commun., 2012, 48, 11781
DOI: 10.1039/C2CC36352F

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