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Issue 4, 2012
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Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

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Abstract

We describe herein the use of glycerol as the solvent in the copper-catalyzed cross-coupling reaction of diaryl diselenides with arylboronic acids using CuI and DMSO as additive. This cross-coupling reaction was performed with diaryl diselenides and arylboronic acids bearing electron-withdrawing and electron-donating groups, affording the corresponding diaryl selenides in good to excellent yields. The glycerol–CuI mixture can be directly reused for further cross-coupling reactions.

Graphical abstract: Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

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Article information


Submitted
10 Nov 2011
Accepted
13 Jan 2012
First published
24 Feb 2012

Green Chem., 2012,14, 1030-1034
Article type
Paper

Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

V. G. Ricordi, C. S. Freitas, G. Perin, E. J. Lenardão, R. G. Jacob, L. Savegnago and D. Alves, Green Chem., 2012, 14, 1030
DOI: 10.1039/C2GC16427B

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