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Issue 4, 2012
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Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

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Abstract

We describe herein the use of glycerol as the solvent in the copper-catalyzed cross-coupling reaction of diaryl diselenides with arylboronic acids using CuI and DMSO as additive. This cross-coupling reaction was performed with diaryl diselenides and arylboronic acids bearing electron-withdrawing and electron-donating groups, affording the corresponding diaryl selenides in good to excellent yields. The glycerol–CuI mixture can be directly reused for further cross-coupling reactions.

Graphical abstract: Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

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Publication details

The article was received on 10 Nov 2011, accepted on 13 Jan 2012 and first published on 24 Feb 2012


Article type: Paper
DOI: 10.1039/C2GC16427B
Green Chem., 2012,14, 1030-1034

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    Glycerol as a recyclable solvent for copper-catalyzed cross-coupling reactions of diaryl diselenides with aryl boronic acids

    V. G. Ricordi, C. S. Freitas, G. Perin, E. J. Lenardão, R. G. Jacob, L. Savegnago and D. Alves, Green Chem., 2012, 14, 1030
    DOI: 10.1039/C2GC16427B

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