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Issue 4, 2011
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Scalable synthesis of catalysts for the Mizoroki–Heck cross coupling reaction: palladium nanoparticles assembled in a polymeric nanosphere

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Abstract

Palladium nano-spheres 160 nm in diameter, as an assembly of uniform 5 nm nanoparticles, are accessible using a facile one step method under continuous flow on a spinning disc with hydrogen gas as the reducing agent. The stable colloidal system is an effective catalyst for the Mizoroki–Heck reaction, as established for the reaction between several aryl halides and n-butyl acrylate, and can be readily recycled without a change in their catalytic activity.

Graphical abstract: Scalable synthesis of catalysts for the Mizoroki–Heck cross coupling reaction: palladium nanoparticles assembled in a polymeric nanosphere

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Publication details

The article was received on 15 Nov 2010, accepted on 06 Jan 2011 and first published on 09 Feb 2011


Article type: Paper
DOI: 10.1039/C0NJ00898B
Citation: New J. Chem., 2011,35, 854-860
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    Scalable synthesis of catalysts for the Mizoroki–Heck cross coupling reaction: palladium nanoparticles assembled in a polymeric nanosphere

    J. Zou, K. Swaminathan Iyer, S. G. Stewart and C. L. Raston, New J. Chem., 2011, 35, 854
    DOI: 10.1039/C0NJ00898B

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