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Issue 36, 2011
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Synthesis and X-ray crystal structure of a difunctionalized pillar[5]arene at A1/B2 positions by in situcyclization and deprotection

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Abstract

The reaction of 1,4-dimethoxybenzene and paraformaldehyde using AlBr3 yields multiple-deprotected pillar[5]arenes. A1/B2 di-deprotected pillar[5]arene can be isolated by silica gel chromatography and washing procedures. The X-ray structure and polymerization of the A1/B2 di-deprotected pillar[5]arene are reported.

Graphical abstract: Synthesis and X-ray crystal structure of a difunctionalized pillar[5]arene at A1/B2 positions by in situcyclization and deprotection

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Publication details

The article was received on 15 Jun 2011, accepted on 18 Jul 2011 and first published on 03 Aug 2011


Article type: Communication
DOI: 10.1039/C1CC13546E
Chem. Commun., 2011,47, 10106-10108

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    Synthesis and X-ray crystal structure of a difunctionalized pillar[5]arene at A1/B2 positions by in situcyclization and deprotection

    T. Ogoshi, K. Kitajima, S. Fujinami and T. Yamagishi, Chem. Commun., 2011, 47, 10106
    DOI: 10.1039/C1CC13546E

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