Issue 8, 2011
From the journal:

Physical Chemistry Chemical Physics

BET specific surface area and pore structure of MOFs determined by hydrogen adsorption at 20 K†

Barbara Streppela  and  Michael Hirscher*a  

* Corresponding authors

a Max Planck Institute for Metals Research, Heisenbergstr. 3, 70569 Stuttgart, Germany
E-mail: hirscher@mf.mpg.de
Fax: +49 711 6891952
Tel: +49 711 6891808

Abstract

Low-pressure high-resolution hydrogen adsorption for the metal–organic framework MIL-101 are measured at 19.5 K and pressures below 57 kPa. The BET specific surface area and micropore volume are determined and compared to results from nitrogen adsorption at 77 K. Steps in the hydrogen adsorption isotherm are correlated to the pore structure of MIL-101.

Graphical abstract: BET specific surface area and pore structure of MOFs determined by hydrogen adsorption at 20 K

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Article information

DOI
https://doi.org/10.1039/C0CP01873B
Article type
Communication
Submitted
20 Sep 2010
Accepted
17 Nov 2010
First published
22 Dec 2010

Phys. Chem. Chem. Phys., 2011,13, 3220-3222

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BET specific surface area and pore structure of MOFs determined by hydrogen adsorption at 20 K

B. Streppel and M. Hirscher, Phys. Chem. Chem. Phys., 2011, 13, 3220 DOI: 10.1039/C0CP01873B

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