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Abstract | Cited by

Controlled dispersion nitroxide mediated polymerization (NMP) of methyl methacrylate (MMA) was successfully carried out in supercritical carbon dioxide (scCO2) in the presence of a CO2-philic perfluorinated stabilizer generated “in situ”. This is an efficient green approach for preparing free flowing PMMA powder consisting of small sized microspheres.

Graphical abstract: Dispersion nitroxide mediated polymerization of methyl methacrylate in supercritical carbon dioxide using in situ formed stabilizers

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