Issue 3, 2010
From the journal:

Organic & Biomolecular Chemistry

A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers†

Kamyar Afarinkia,*a   Martin Royappa,a   Ian J. Scowen,b   Jonathan W. Steedc  and  Hiu-wan Yua  

* Corresponding authors

a Institute of Cancer Therapeutics, Thumbling Hill Street, Bradford, UK
E-mail: k.afarinkia@bradford.ac.uk
Fax: +44 (0)1274 233234
Tel: +44 (0)1274 235831

b Analytical Center, University of Bradford, Bradford, UK
E-mail: i.scowen@bradford.ac.uk
Fax: +44 (0)1274 233234
Tel: +44 (0)1274 23619

c Department of Chemistry, University of Durham, Durham, UK
E-mail: jon.steed@durham.ac.uk
Tel: +44 (0)191 33 42085

Abstract

A general method for the synthesis of a novel class of oligomers, comprising α-hydroxy phenylphosphinic acid building blocks, is reported. A series of dimeric α-hydroxy phenylphosphinates are analyzed by a combination of NMR spectroscopy, X-ray crystallography and computational methods.

Graphical abstract: A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers

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Article information

DOI
https://doi.org/10.1039/B917737J
Article type
Paper
Submitted
28 Aug 2009
Accepted
30 Oct 2009
First published
03 Dec 2009

Org. Biomol. Chem., 2010,8, 600-606

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A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers

K. Afarinkia, M. Royappa, I. J. Scowen, J. W. Steed and H. Yu, Org. Biomol. Chem., 2010, 8, 600 DOI: 10.1039/B917737J

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