Issue 3, 2010
From the journal:

New Journal of Chemistry

An improved two-step synthetic route to primary allylic alcohols from aldehydes†

Zheng Liu,a   Yaqiong Gong,a   Hoe-Sup Byuna  and  Robert Bittman*a  

* Corresponding authors

a Department of Chemistry and Biochemistry, Queens College of The City University of New York, Flushing, USA
E-mail: robert.bittman@qc.cuny.edu

Abstract

An improved two-step synthetic route to allylic alcohols from aldehydes has been developed. A modification of the HWE reaction in H2O–2-PrOH (1 ∶ 1) and a convenient protocol to prepare AlH3 in THF from LiAlH4 and n-BuBr are the key factors in the improvement.

Graphical abstract: An improved two-step synthetic route to primary allylic alcohols from aldehydes

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Article information

DOI
https://doi.org/10.1039/B9NJ00710E
Article type
Paper
Submitted
25 Nov 2009
Accepted
02 Dec 2009
First published
12 Jan 2010

New J. Chem., 2010,34, 470-475

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An improved two-step synthetic route to primary allylic alcohols from aldehydes

Z. Liu, Y. Gong, H. Byun and R. Bittman, New J. Chem., 2010, 34, 470 DOI: 10.1039/B9NJ00710E

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