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Reaction of Na2WO4 and NaVO3 with cis-Ru(dmso)4Cl2 in buffer solution (pH 6) led to the formation of a novel polyanion [HVW7O28Ru(dmso)3]6− (1), which is composed of an unprecedented heptatungstovanadate fragment stabilized by one Ru(dmso)3 group. The crystallization of 1 with sodium–potassium resulted in Na4K2[HVW7O28Ru(dmso)3]·Na3VO4·15H2O (1a), which exhibits a 3D architecture formed by the polyanion 1 and sodium–potassium linkers. and sodium–potassium linkers.

Graphical abstract: A novel heptatungstovanadate fragment stabilized by organo-ruthenium group: [HVW7O28Ru(dmso)3]6−

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