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Issue 6, 2010
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H-bonding schemes of di- and tri-p-benzamides assessed by a combination of electron diffraction, X-ray powder diffraction and solid-state NMR

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Abstract

The crystal structures of di- and tri-p-benzamides are solved by a combination of single crystal, electron and powder X-ray diffraction. Different hydrogen-bonding schemes observed in the two structures are described and classified. The hydrogen-bonding networks are correlated to complementary data obtained from multinuclear solid-state NMR.

Graphical abstract: H-bonding schemes of di- and tri-p-benzamides assessed by a combination of electron diffraction, X-ray powder diffraction and solid-state NMR

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Supplementary files

Article information


Submitted
02 Oct 2009
Accepted
15 Jan 2010
First published
28 Jan 2010

CrystEngComm, 2010,12, 1824-1832
Article type
Paper

H-bonding schemes of di- and tri-p-benzamides assessed by a combination of electron diffraction, X-ray powder diffraction and solid-state NMR

T. Gorelik, G. Matveeva, U. Kolb, T. Schleuß, A. F. M. Kilbinger, J. van de Streek, A. Bohle and G. Brunklaus, CrystEngComm, 2010, 12, 1824
DOI: 10.1039/B920569A

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