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Issue 40, 2010
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Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

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Abstract

Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal–organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.

Graphical abstract: Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

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Supplementary files

Article information


Submitted
17 Jul 2010
Accepted
27 Aug 2010
First published
17 Sep 2010

Chem. Commun., 2010,46, 7572-7574
Article type
Communication

Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

K. Fujii, A. L. Garay, J. Hill, E. Sbircea, Z. Pan, M. Xu, D. C. Apperley, S. L. James and K. D. M. Harris, Chem. Commun., 2010, 46, 7572
DOI: 10.1039/C0CC02635B

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