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Issue 18, 2009
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Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

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Abstract

A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50%-U-13C-CsC60.

Graphical abstract: Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

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Supplementary files

Article information


Submitted
24 Oct 2008
Accepted
26 Jan 2009
First published
02 Mar 2009

Phys. Chem. Chem. Phys., 2009,11, 3547-3553
Article type
Paper

Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

D. Lee, J. Struppe, D. W. Elliott, L. J. Mueller and J. J. Titman, Phys. Chem. Chem. Phys., 2009, 11, 3547
DOI: 10.1039/B818867J

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