Issue 11, 2009
From the journal:

Chemical Communications

A systematic approach to the generation of long-lived metal alkane complexes: combined IR and NMR study of (Tp)Re(CO)2(cyclopentane)†

Simon B. Duckett,*a   Michael W. George,*b   Omar S. Jina,b   Steven L. Matthews,a   Robin N. Perutz,*a   Xue-Zhong Sunb  and  Khuong Q. Vuongb  

* Corresponding authors

a Department of Chemistry, University of York, Heslington, York, UK
E-mail: rnp1@york.ac.uk
Fax: +44 (0)1904 432516
Tel: +44 (0)1904 432549

b School of Chemistry, University of Nottingham, University Park, Nottingham, UK
E-mail: mike.george@nottingham.ac.uk
Fax: +44 (0)115 9513563
Tel: +44 (0)115 9513512

Abstract

Short wavelength photolysis of (Tp)Re(CO)3 (Tp = tris(pyrazol-1-yl)borate) at low-temperature in cyclopentane yielded (Tp)Re(CO)2(cyclopentane), an alkane complex with three nitrogen ligands that was characterised by NMR spectroscopy.

Graphical abstract: A systematic approach to the generation of long-lived metal alkane complexes: combined IR and NMR study of (Tp)Re(CO)2(cyclopentane)

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Article information

DOI
https://doi.org/10.1039/B819671K
Article type
Communication
Submitted
05 Nov 2008
Accepted
17 Dec 2008
First published
21 Jan 2009

Chem. Commun., 2009, 1401-1403

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A systematic approach to the generation of long-lived metal alkane complexes: combined IR and NMR study of (Tp)Re(CO)2(cyclopentane)

S. B. Duckett, M. W. George, O. S. Jina, S. L. Matthews, R. N. Perutz, X. Sun and K. Q. Vuong, Chem. Commun., 2009, 1401 DOI: 10.1039/B819671K

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