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Abstract | Cited by

When isolated in the high vacuum of an ESI-FTICR mass spectrometer, bowl-shaped metallo-supramolecular M6L4 assemblies undergo a surprising and mechanistically interesting intramolecular double cage contraction to yield smaller M3L2 cages.

Graphical abstract: A double intramolecular cage contraction within a self-assembled metallo-supramolecular bowl

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