Issue 5, 2008
From the journal:

Organic & Biomolecular Chemistry

Glycosidations of 2-deoxy glycosyl dithiophosphates using a tagged iodine(iii)-promoter for simple purification

Eike Kunst,a   Florian Gallier,ab   Gilles Dujardinb  and  Andreas Kirschning*a  

* Corresponding authors

a Institut für Organische Chemie and Zentrum für Biomolekulare Wirkstoffe (BMWZ), Leibniz Universität Hannover, Schneiderberg 1b, 30167 Hannover, Germany
E-mail: andreas.kirschning@oci.uni-hannover.de
Fax: +49 (0)511-7623011

b UCO2M, UMR CNRS 6011, Université du Maine, F-72085 Le Mans Cedex 9, France

Abstract

The preparation of the 4-i-butylsulfonate derivative of the Zefirov reagent (5) and its use in a novel purification strategy for iodine(III)-promoted glycosidations of 2-deoxy diethyldithiophosphate glycosides is described.

Graphical abstract: Glycosidations of 2-deoxy glycosyl dithiophosphates using a tagged iodine(iii)-promoter for simple purification

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Article information

DOI
https://doi.org/10.1039/B718642H
Article type
Paper
Submitted
03 Dec 2007
Accepted
03 Jan 2008
First published
24 Jan 2008

Org. Biomol. Chem., 2008,6, 893-898

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Glycosidations of 2-deoxy glycosyl dithiophosphates using a tagged iodine(III)-promoter for simple purification

E. Kunst, F. Gallier, G. Dujardin and A. Kirschning, Org. Biomol. Chem., 2008, 6, 893 DOI: 10.1039/B718642H

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